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Wereport on asynchronization ofsynchrotron radiation source“KSSR-Kurchatov”with sub-PW femtosecond laser using developed active phaselocking system with integrated proportional-integral-derivativecontroller forcompensating both phasejitterand drift. Thestability ofthesystempaves the way to performlong-term pump-probe X-ray opticalexperiments with atemporalresolution about 30 ps inNRC «Kurchatov Institute»